_audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C0.04 O3.83 Si1.92' _chemical_formula_weight 115.67 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system cubic _space_group_IT_number 218 _space_group_name_H-M_alt 'P -4 3 n' _space_group_name_Hall 'P -4n 2 3' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'x, -y, -z' '-x, y, -z' 'z, x, y' 'y, z, x' '-z, -x, y' '-y, z, -x' 'z, -x, -y' '-y, -z, x' '-z, x, -y' 'y, -z, -x' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' '-y+1/2, x+1/2, -z+1/2' 'y+1/2, -x+1/2, -z+1/2' 'x+1/2, z+1/2, y+1/2' 'z+1/2, y+1/2, x+1/2' '-x+1/2, -z+1/2, y+1/2' 'z+1/2, -y+1/2, -x+1/2' '-x+1/2, z+1/2, -y+1/2' '-z+1/2, -y+1/2, x+1/2' 'x+1/2, -z+1/2, -y+1/2' '-z+1/2, y+1/2, -x+1/2' _cell_length_a 13.406(2) _cell_length_b 13.406(2) _cell_length_c 13.406(2) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2409.3(11) _cell_formula_units_Z 24 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 450 _cell_measurement_theta_min 2.32 _cell_measurement_theta_max 45.85 _exptl_crystal_description cube _exptl_crystal_colour ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.913 _exptl_crystal_F_000 1386 _exptl_transmission_factor_min 0.5863 _exptl_transmission_factor_max 0.7454 _exptl_crystal_size_max 0.31 _exptl_crystal_size_mid 0.28 _exptl_crystal_size_min 0.25 _exptl_absorpt_coefficient_mu 0.716 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details 'SADABS (Bruker, 2008)' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker SMART CCD' _diffrn_measurement_method '\w scan' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 20241 _diffrn_reflns_av_unetI/netI 0.0422 _diffrn_reflns_av_R_equivalents 0.1055 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 2.148 _diffrn_reflns_theta_max 26.634 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 858 _reflns_number_gt 733 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.762 _reflns_Friedel_fraction_max 1.000 _reflns_Friedel_fraction_full 1.000 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refined as a 2-component perfect inversion twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+34.0716P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Refined as a perfect inversion twin. ; _refine_ls_abs_structure_Flack 0.5 _chemical_absolute_configuration ? _refine_ls_number_reflns 858 _refine_ls_number_parameters 63 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0856 _refine_ls_R_factor_gt 0.0748 _refine_ls_wR_factor_ref 0.1698 _refine_ls_wR_factor_gt 0.1650 _refine_ls_goodness_of_fit_ref 1.120 _refine_ls_restrained_S_all 1.120 _refine_ls_shift/su_max 1.351 _refine_ls_shift/su_mean 0.225 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si 0.3170(3) 0.3170(3) 0.3170(3) 0.0222(15) Uani 1 3 d S T P . . Si2 Si 0.1827(4) 0.1827(4) 0.1827(4) 0.0299(16) Uani 1 3 d S T P . . Si3 Si 0.0000 0.2500 0.5000 0.0221(12) Uani 1 4 d S T P . . Si4 Si 0.0005(4) 0.1141(2) 0.3102(2) 0.0292(9) Uani 1 1 d . . . . . O1 O 0.0000 0.0000 0.3433(7) 0.039(3) Uani 1 2 d S T P . . O2 O 0.2549(16) 0.2549(16) 0.2549(16) 0.072(6) Uani 1 3 d S T P . . O3 O 0.0972(14) 0.1348(13) 0.2426(16) 0.071(5) Uani 1 1 d . . . . . O4 O 0.3650(16) 0.4029(12) 0.2500(15) 0.071(5) Uani 1 1 d . . . . . O5 O -0.0168(13) 0.1826(8) 0.4071(7) 0.061(4) Uani 1 1 d . . . . . Q1 C 0.2500 0.0000 0.5000 1(314) Uiso 0.0(9) 4 d S . . . . Q2 C 0.264(5) -0.024(6) 0.440(4) 0.17(4) Uiso 0.78(13) 1 d . . . . . Q3 C 0.5000 0.5000 0.5000 0.3(2) Uiso 0.6(3) 12 d S . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0222(15) 0.0222(15) 0.0222(15) -0.0027(17) -0.0027(17) -0.0027(17) Si2 0.0299(16) 0.0299(16) 0.0299(16) 0.004(2) 0.004(2) 0.004(2) Si3 0.0259(18) 0.014(2) 0.0259(18) 0.000 0.000 0.000 Si4 0.0360(17) 0.0315(16) 0.0201(14) -0.0011(12) 0.007(3) 0.024(2) O1 0.054(8) 0.035(7) 0.030(6) 0.000 0.000 0.027(11) O2 0.072(6) 0.072(6) 0.072(6) -0.027(5) -0.027(5) -0.027(5) O3 0.082(13) 0.037(8) 0.094(12) 0.015(9) 0.033(10) -0.011(9) O4 0.090(13) 0.058(9) 0.064(11) 0.041(8) 0.015(10) -0.010(10) O5 0.087(12) 0.058(6) 0.037(5) -0.025(5) -0.005(7) -0.008(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si1 O4 1.596(15) 6 ? Si1 O4 1.596(14) 5 ? Si1 O4 1.596(15) . ? Si1 O2 1.45(4) . ? Si2 O2 1.66(4) . ? Si2 O3 1.540(16) 6 ? Si2 O3 1.540(16) 5 ? Si2 O3 1.540(16) . ? Si3 O5 1.556(9) . ? Si3 O5 1.556(9) 22 ? Si3 O5 1.556(9) 4_556 ? Si3 O5 1.556(9) 20_455 ? Si4 O3 1.606(18) . ? Si4 O1 1.592(4) . ? Si4 O4 1.562(15) 16_455 ? Si4 O5 1.607(10) . ? O1 Si4 1.592(4) 2 ? O4 Si4 1.562(15) 15 ? Q1 Q2 0.89(4) 3_556 ? Q1 Q2 0.89(4) 21_545 ? Q1 Q2 0.89(4) 19 ? Q1 Q2 0.89(4) . ? Q2 Q2 1.29(7) 21_545 ? Q2 Q2 1.29(7) 19 ? Q2 Q2 1.74(8) 3_556 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 Si1 O4 110.0(8) 6 5 ? O4 Si1 O4 110.0(8) 6 . ? O4 Si1 O4 110.0(8) 5 . ? O4 Si1 O2 108.7(8) 6 . ? O4 Si1 O2 109.2(8) 5 . ? O4 Si1 O2 108.8(8) . . ? O2 Si2 O3 111.8(9) . 6 ? O2 Si2 O3 111.4(9) . 5 ? O3 Si2 O3 107.2(10) 6 5 ? O2 Si2 O3 111.9(9) . . ? O3 Si2 O3 107.2(10) 6 . ? O3 Si2 O3 107.2(10) 5 . ? O5 Si3 O5 109.7(4) . 22 ? O5 Si3 O5 108.9(9) . 4_556 ? O5 Si3 O5 109.7(4) 22 4_556 ? O5 Si3 O5 109.7(4) . 20_455 ? O5 Si3 O5 108.9(9) 22 20_455 ? O5 Si3 O5 109.7(4) 4_556 20_455 ? O3 Si4 O1 109.0(7) . . ? O3 Si4 O4 110.7(6) . 16_455 ? O1 Si4 O4 108.3(9) . 16_455 ? O3 Si4 O5 118.3(10) . . ? O1 Si4 O5 108.9(6) . . ? O4 Si4 O5 101.2(10) 16_455 . ? Si4 O1 Si4 147.7(7) . 2 ? Si2 O2 Si1 179.4(3) . . ? Si4 O3 Si2 165.3(13) . . ? Si1 O4 Si4 165.3(15) . 15 ? Si3 O5 Si4 163.4(13) . . ? Q2 Q1 Q2 92.7(19) 3_556 21_545 ? Q2 Q1 Q2 92.7(19) 3_556 19 ? Q2 Q1 Q2 155(9) 21_545 19 ? Q2 Q1 Q2 155(9) 3_556 . ? Q2 Q1 Q2 92.7(19) 21_545 . ? Q2 Q1 Q2 92.7(19) 19 . ? Q1 Q2 Q2 43.6(9) . 21_545 ? Q1 Q2 Q2 43.6(9) . 19 ? Q2 Q2 Q2 85(3) 21_545 19 ? Q1 Q2 Q2 13(4) . 3_556 ? Q2 Q2 Q2 47.6(17) 21_545 3_556 ? Q2 Q2 Q2 47.6(17) 19 3_556 ? _refine_diff_density_max 0.569 _refine_diff_density_min -0.531 _refine_diff_density_rms 0.133 _shelx_res_file ; D:\Uni\Tribaudino\melanoflogite\SCr\MEP_Aut\mep_aut.res created by SHELXL-2014/7 REM REM Shelx file produced by Sir2011 on Mon Jul 11 2016 at 09:48:54 REM Structure name: PR_A REM TITL Sir2011_AG_RT 11/07/2016 CELL 0.71073 13.406 13.406 13.406 90.0000 90.0000 90.0000 ZERR 24 0.002 0.002 0.002 0.0000 0.0000 0.0000 LATT -1 SYMM -X,-Y,Z SYMM X,-Y,-Z SYMM -X,Y,-Z SYMM Z,X,Y SYMM Y,Z,X SYMM -Z,-X,Y SYMM -Y,Z,-X SYMM Z,-X,-Y SYMM -Y,-Z,X SYMM -Z,X,-Y SYMM Y,-Z,-X SYMM 1/2+Y,1/2+X,1/2+Z SYMM 1/2-Y,1/2-X,1/2+Z SYMM 1/2-Y,1/2+X,1/2-Z SYMM 1/2+Y,1/2-X,1/2-Z SYMM 1/2+X,1/2+Z,1/2+Y SYMM 1/2+Z,1/2+Y,1/2+X SYMM 1/2-X,1/2-Z,1/2+Y SYMM 1/2+Z,1/2-Y,1/2-X SYMM 1/2-X,1/2+Z,1/2-Y SYMM 1/2-Z,1/2-Y,1/2+X SYMM 1/2+X,1/2-Z,1/2-Y SYMM 1/2-Z,1/2+Y,1/2-X SFAC O SI C UNIT 92 46 1 OMIT 0 MERG 2 BOND ACTA TWIN L.S. 8 FMAP 2 PLAN 25 WGHT 0.000000 34.071598 FVAR 0.33726 0.90000 SI1 2 0.317038 0.317038 0.317038 10.33333 0.02220 0.02220 = 0.02220 -0.00268 -0.00268 -0.00268 SI2 2 0.182720 0.182720 0.182720 10.33333 0.02987 0.02987 = 0.02987 0.00356 0.00356 0.00356 SI3 2 0.000000 0.250000 0.500000 10.25000 0.02594 0.01431 = 0.02594 0.00000 0.00000 0.00000 SI4 2 0.000451 0.114069 0.310223 11.00000 0.03597 0.03154 = 0.02006 -0.00109 0.00679 0.02438 O1 1 0.000000 0.000000 0.343277 10.50000 0.05356 0.03473 = 0.02959 0.00000 0.00000 0.02653 O2 1 0.254880 0.254880 0.254880 10.33333 0.07232 0.07232 = 0.07232 -0.02727 -0.02727 -0.02727 O3 1 0.097208 0.134752 0.242627 11.00000 0.08189 0.03681 = 0.09412 0.01531 0.03340 -0.01091 O4 1 0.364972 0.402929 0.249965 11.00000 0.08983 0.05762 = 0.06429 0.04121 0.01512 -0.00988 O5 1 -0.016816 0.182570 0.407080 11.00000 0.08711 0.05778 = 0.03724 -0.02457 -0.00545 -0.00835 Q1 3 0.250000 0.000000 0.500000 -2.08524 1.31464 Q2 3 0.264451 -0.023924 0.439629 0.78372 0.17408 Q3 3 0.500000 0.500000 0.500000 0.04941 0.25133 HKLF 4 REM Sir2011_AG_RT 11/07/2016 REM R1 = 0.0748 for 733 Fo > 4sig(Fo) and 0.0856 for all 858 data REM 63 parameters refined using 0 restraints END WGHT 0.0125 26.8383 REM Highest difference peak 0.569, deepest hole -0.531, 1-sigma level 0.133 Q1 1 0.0000 0.0000 0.1961 10.50000 0.05 0.57 Q2 1 0.0500 0.1971 0.3870 11.00000 0.05 0.44 Q3 1 0.3991 0.4413 0.2335 11.00000 0.05 0.42 Q4 1 0.1165 0.1627 0.3024 11.00000 0.05 0.41 Q5 1 0.2867 0.3895 0.2734 11.00000 0.05 0.40 Q6 1 0.2375 0.2219 0.1257 11.00000 0.05 0.40 Q7 1 0.0515 0.0064 0.3240 11.00000 0.05 0.40 Q8 1 0.3183 0.4151 0.2042 11.00000 0.05 0.39 Q9 1 0.0297 0.1976 0.4161 11.00000 0.05 0.39 Q10 1 0.2987 -0.1438 0.3496 11.00000 0.05 0.39 Q11 1 -0.0491 0.2124 0.4207 11.00000 0.05 0.39 Q12 1 0.3998 0.4238 0.2495 11.00000 0.05 0.38 Q13 1 0.3260 0.3312 0.1565 11.00000 0.05 0.38 Q14 1 0.0027 0.1598 0.1467 11.00000 0.05 0.38 Q15 1 0.6212 0.4600 0.5374 11.00000 0.05 0.37 Q16 1 0.1761 0.1512 0.2415 11.00000 0.05 0.37 Q17 1 0.2669 0.3211 0.2453 11.00000 0.05 0.36 Q18 1 -0.0737 0.0991 0.3524 11.00000 0.05 0.36 Q19 1 0.1835 0.1669 0.3542 11.00000 0.05 0.36 Q20 1 0.0706 0.1294 0.3066 11.00000 0.05 0.35 Q21 1 -0.0356 0.1927 0.4383 11.00000 0.05 0.35 Q22 1 0.2612 -0.0040 0.2796 11.00000 0.05 0.34 Q23 1 0.0525 0.0217 0.2518 11.00000 0.05 0.33 Q24 1 0.4468 0.3770 0.2039 11.00000 0.05 0.33 Q25 1 0.0814 0.1515 0.2104 11.00000 0.05 0.33 ; _shelx_res_checksum 83815 _shelx_hkl_file ; 0 0 1 -1.6998 0.9670 1 1 0 0 -1.5549 1.1674 1 0 0 1 -1.7607 1.0030 2 0 0 -1 -0.9843 0.7948 3 0 -1 0 -2.2245 0.7295 2 1 0 0 -0.6611 1.0163 2 1 0 0 -1.5109 0.9594 3 0 1 0 -1.4252 1.1870 1 0 -1 0 -0.2338 0.9006 3 -1 0 1 60.2903 7.0607 2 1 -1 0 63.7707 7.1887 2 0 -1 1 40.4432 6.9625 2 1 0 1 48.8693 7.6288 1 1 0 1 42.9400 7.0961 2 0 -1 1 62.4968 6.8512 3 0 -1 -1 60.0553 6.7907 3 0 1 1 68.8607 7.6103 1 0 1 1 64.2997 7.0343 2 1 -1 0 62.2520 6.8611 3 1 0 -1 67.3754 7.0187 3 0 1 -1 62.9298 7.4492 1 1 1 0 52.2185 7.5274 1 -1 1 0 54.5102 7.4621 1 -1 1 1 -10.324 1.640 2 1 1 -1 -10.445 1.732 1 -1 1 1 -11.854 1.709 1 1 -1 1 -12.104 1.895 2 -1 -1 -1 -7.9652 1.2714 3 1 -1 1 -10.900 1.268 3 -1 -1 1 -12.176 1.386 3 1 1 1 -9.6800 2.2554 1 1 -1 -1 -6.1362 1.7508 3 -1 1 -1 -10.989 1.728 1 1 1 1 -8.9528 1.6752 2 -1 -1 1 -11.550 1.364 2 0 2 0 1311.86 153.35 1 0 0 -2 1261.80 141.13 3 0 -2 0 1197.93 145.09 2 2 0 0 1210.95 153.32 1 2 0 0 1220.93 141.19 3 0 -2 0 1390.08 141.23 3 0 0 2 1231.29 145.27 2 2 0 0 1224.66 145.23 2 0 0 2 1282.78 153.22 1 0 -2 1 2053.70 228.82 3 2 1 0 2018.33 235.22 2 2 1 0 1847.36 228.78 3 2 -1 0 2067.26 235.40 2 0 -2 -1 2104.19 228.81 3 1 0 2 2085.18 235.40 2 0 2 1 2022.75 235.22 2 1 0 2 2378.90 248.52 1 2 1 0 2007.79 248.41 1 -2 1 0 1988.75 248.30 1 1 0 -2 1932.62 228.84 3 0 2 -1 2021.33 248.36 1 0 2 1 2177.54 248.44 1 0 -2 1 2043.61 235.26 2 2 -1 0 1941.33 228.80 3 2 0 1 1930.06 224.32 3 -1 2 0 2047.12 243.64 1 0 1 -2 2105.09 243.50 1 0 1 2 2031.54 243.57 1 1 2 0 1977.79 243.69 1 2 0 -1 2046.55 224.52 3 -2 0 1 2085.21 230.80 2 1 -2 0 2044.19 224.46 3 0 -1 2 1905.64 224.36 3 0 -1 2 2109.30 230.89 2 2 0 1 1747.03 243.69 1 -1 -2 0 2048.60 224.43 3 0 1 2 2028.76 230.85 2 0 -1 -2 2050.19 224.38 3 2 0 1 2053.49 230.89 2 1 -2 0 2009.48 230.84 2 2 0 -1 1846.09 243.50 1 1 -2 1 2295.90 246.08 3 2 -1 1 2266.56 245.99 3 1 -2 1 2160.29 253.11 2 1 2 -1 2329.46 267.11 1 1 1 -2 2391.64 246.15 3 -2 1 1 2264.32 266.96 1 -1 2 1 2279.82 253.05 2 -1 1 2 2030.12 253.08 2 1 -1 2 2073.54 245.92 3 -1 1 2 2139.64 266.94 1 2 1 -1 2315.58 246.17 3 -1 2 1 2314.07 267.11 1 1 -1 2 2125.91 253.14 2 2 1 -1 2137.95 267.00 1 2 -1 1 2149.25 253.17 2 -2 -1 -1 2135.80 245.94 3 -1 1 -2 2257.89 267.04 1 1 -2 -1 2258.74 246.11 3 1 1 2 2400.10 267.22 1 1 2 1 2044.47 267.15 1 -2 1 -1 2099.96 267.05 1 -1 -2 1 2353.11 246.11 3 2 1 1 1992.06 267.19 1 2 -1 -1 2246.31 253.13 2 2 1 1 2247.59 253.03 2 2 -1 -1 2126.34 246.13 3 -1 -2 1 2146.11 252.89 2 -1 2 -1 2065.90 267.08 1 1 2 1 1971.91 252.91 2 1 -1 -2 2223.08 246.12 3 1 1 2 2269.19 253.10 2 -2 -1 1 2218.44 252.96 2 2 0 -2 71.8103 6.7398 3 2 -2 0 50.6675 6.6005 2 0 -2 -2 46.3630 5.9946 3 0 2 -2 47.6149 6.5338 1 0 -2 2 44.8504 6.0258 3 2 -2 0 46.9584 6.1338 3 2 0 2 40.0457 6.5181 2 0 2 2 55.9762 6.3699 2 -2 2 0 53.9119 6.8069 1 -2 0 2 44.4457 6.2769 2 2 0 2 58.4357 7.5923 1 2 2 0 54.8479 7.1022 1 0 2 2 40.6494 6.9519 1 0 -2 2 10.9939 5.9229 2 2 -1 2 -1.8409 3.3669 1 -2 1 2 6.22635 2.08552 1 2 -2 1 -1.1746 2.0792 3 -2 2 1 5.59616 2.62372 1 -1 -2 -2 3.95926 2.06136 3 2 -1 2 -1.4327 3.0253 2 -2 -2 -1 2.86937 2.09248 3 -2 -1 -2 2.37027 1.48123 3 2 1 -2 -2.0072 2.6514 3 2 -2 1 1.82216 3.07101 2 -1 2 2 -2.0316 2.8921 1 1 -2 2 3.12999 2.90452 2 -2 1 2 -2.4691 2.1438 2 1 -2 2 -3.0622 2.0145 3 2 2 -1 -1.4781 2.7381 1 -1 2 2 1.41665 2.35924 2 2 1 -2 3.79046 2.16243 1 1 2 -2 -1.6948 2.7616 1 2 -1 2 -1.0233 1.5974 3 2 -2 -1 0.03640 2.43485 2 2 2 1 1.80508 2.15346 2 -1 -2 2 -1.2067 2.2647 2 -2 2 -1 -1.4531 2.6418 1 -2 -1 2 2.20903 2.23635 2 1 -2 -2 1.22207 2.39214 3 2 -1 -2 1.08554 2.66576 3 2 1 2 2.85155 2.82285 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219.575 27.893 2 8 -4 3 214.012 26.654 3 -4 3 8 179.624 28.598 2 4 -3 8 201.441 28.831 2 -8 4 3 252.609 28.716 2 3 -8 4 206.084 28.705 2 -8 4 3 205.773 29.384 1 3 -8 4 231.253 27.417 3 8 -4 3 189.901 28.657 2 -3 8 4 222.648 31.173 1 4 3 8 281.626 32.536 1 8 4 3 236.294 31.874 1 -4 -3 8 212.273 29.033 2 8 -4 -3 209.552 27.794 3 -4 -3 8 226.804 27.163 3 -4 3 -8 243.959 29.870 1 3 8 4 178.371 31.155 1 -3 8 -4 228.874 30.868 1 -8 4 -3 184.087 29.799 1 4 -3 -8 218.326 28.249 3 8 4 3 268.028 28.270 2 4 3 8 217.161 29.032 2 3 8 4 197.194 27.331 2 -8 -4 3 207.236 27.309 3 -3 -8 4 229.768 27.808 3 3 -8 -4 225.812 27.678 3 -3 -8 4 242.803 27.184 2 -8 -4 3 202.393 27.084 2 8 5 -3 1042.51 130.08 1 -8 5 3 1099.65 129.50 1 8 -5 3 1017.57 118.94 3 5 -3 8 1041.25 118.20 3 -3 8 5 1057.73 130.13 1 3 8 -5 1079.88 129.96 1 3 -8 5 1093.31 123.45 2 -3 -8 -5 991.109 119.192 3 -3 8 5 1069.69 122.87 2 3 -8 5 1068.39 119.35 3 -8 -5 -3 1056.99 119.00 3 5 -3 8 989.117 123.295 2 -5 3 8 985.294 123.175 2 8 -5 3 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34.153 2 -4 -8 0 250.515 32.761 3 0 -4 -8 344.009 32.910 3 4 -8 0 271.105 33.951 2 -8 0 4 285.590 33.697 2 8 0 4 298.867 31.909 3 8 0 -4 243.968 33.121 3 4 -8 0 229.648 32.462 3 8 0 4 265.888 37.159 1 -8 0 4 263.882 34.213 1 -4 8 0 237.890 36.534 1 8 0 4 313.308 34.851 2 0 -4 8 263.696 32.122 3 0 4 8 259.180 36.500 1 4 8 0 244.254 36.053 1 8 -1 4 39.4903 8.5701 3 8 -1 4 1.1327 11.7323 1 -4 8 1 29.5737 11.4169 1 4 -8 1 22.0391 8.6925 3 8 1 -4 24.6634 11.0013 1 -1 -4 -8 28.1735 8.9395 3 4 -8 1 52.5822 10.4136 2 8 1 -4 27.1218 10.1803 3 1 4 -8 48.7916 9.8871 1 8 -1 4 32.3221 10.3878 2 4 8 -1 0.5098 11.1938 1 -1 4 8 41.9517 12.0493 1 -1 4 8 21.1058 10.2565 2 1 -4 8 50.2817 10.5769 2 -8 1 4 39.4994 9.1357 2 -4 -8 -1 52.9175 10.3371 3 1 -4 8 28.4988 7.9257 3 -8 1 4 24.1840 9.1525 1 1 4 8 25.5795 10.7259 2 4 -8 -1 28.8703 9.7677 2 8 1 4 36.2977 13.4355 1 1 -4 -8 27.4745 9.5652 3 8 1 4 40.9319 10.1317 2 8 -1 -4 37.9989 10.3212 3 4 8 1 35.6323 11.9420 1 -4 -8 1 30.0168 9.1424 3 1 4 8 56.7059 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732.073 93.244 1 2 6 8 658.161 86.901 2 -8 2 -6 717.929 91.534 1 -8 -2 6 762.461 87.000 2 6 8 2 724.466 92.761 1 -2 -6 8 624.848 87.138 2 8 2 6 775.320 87.346 2 6 -8 -2 663.180 84.285 3 8 -2 -6 733.287 84.878 3 -2 6 -8 735.200 91.488 1 -6 8 -2 747.640 92.370 1 8 2 6 649.035 93.388 1 -6 -8 2 813.633 84.591 3 8 -3 6 137.281 22.744 2 6 8 -3 179.489 24.457 1 -3 -6 -8 160.862 20.324 3 6 -8 3 159.335 20.611 3 -6 8 3 148.268 21.724 2 8 3 -6 124.453 21.333 3 3 -6 8 160.836 20.235 3 3 6 -8 192.534 23.720 1 8 3 -6 176.278 23.169 1 -6 -8 -3 144.118 21.252 3 8 -3 6 161.130 19.728 3 -3 6 8 125.655 23.528 1 -6 8 3 168.215 24.313 1 3 -6 8 205.938 23.363 2 -3 6 8 116.350 22.102 2 -8 3 6 157.493 22.310 2 6 -8 3 147.266 22.979 2 8 -3 -6 146.443 21.989 3 -3 -6 8 115.197 20.179 3 8 3 6 153.000 22.008 2 8 3 6 142.621 25.417 1 3 6 8 153.760 22.038 2 -3 6 -8 135.236 22.653 1 3 -6 -8 141.865 21.643 3 -6 -8 3 151.882 21.414 3 -3 -6 8 134.295 22.053 2 -8 3 -6 136.023 22.955 1 3 6 8 175.320 25.948 1 6 -8 -3 140.167 21.305 3 -8 -3 6 155.785 21.607 2 -6 8 -3 159.038 24.314 1 6 8 3 124.002 25.240 1 -8 4 6 355.486 43.646 2 6 -8 4 351.527 44.061 2 -6 8 4 357.177 46.799 1 -4 6 8 362.619 43.765 2 -4 6 8 351.289 45.668 1 8 4 -6 327.679 45.419 1 6 8 -4 347.363 45.854 1 4 -6 8 351.151 41.038 3 6 -8 4 369.688 41.453 3 -6 8 4 369.807 43.373 2 8 -4 6 359.073 40.726 3 -6 -8 -4 324.054 41.524 3 4 6 -8 338.853 45.245 1 8 -4 6 312.385 43.764 2 4 -6 8 298.945 43.701 2 4 -6 -8 360.973 42.611 3 -6 8 -4 331.797 46.318 1 -4 6 -8 322.924 45.617 1 -6 -8 4 332.689 42.050 3 4 6 8 295.084 47.297 1 6 8 4 355.088 47.720 1 6 -8 -4 289.127 41.886 3 8 4 6 369.749 43.234 2 -8 4 -6 366.582 46.244 1 -8 -4 6 358.248 43.072 2 8 -4 -6 298.218 42.375 3 -4 -6 8 377.843 42.239 3 -4 -6 8 361.333 43.671 2 -8 -4 6 295.462 41.593 3 4 6 8 411.541 43.739 2 8 4 6 362.157 47.664 1 -6 8 5 1159.60 136.11 2 5 6 -8 1151.54 143.26 1 5 -6 8 1159.78 136.73 2 8 -5 6 1155.71 136.88 2 -6 8 5 1166.98 144.02 1 -5 6 8 1065.60 136.09 2 -6 -8 -5 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49.1042 13.4002 3 2 9 7 31.5089 13.8239 2 7 -2 -9 20.8040 13.3607 3 2 9 7 31.9515 17.1719 1 2 -9 -7 34.7481 12.7294 3 -2 9 -7 63.2918 16.4583 1 7 2 9 28.0504 18.0118 1 7 2 9 45.0722 14.0696 2 -2 -9 7 42.1276 12.1548 3 9 -7 -2 15.6864 12.9432 2 9 7 2 30.3175 18.3357 1 -7 -2 9 -0.5300 14.2164 2 -7 2 -9 54.8559 13.0293 1 -9 -7 2 30.7194 11.6104 3 -9 7 -2 42.4158 15.4416 1 -8 2 9 22.3846 12.6836 2 -2 -9 -8 4.8303 11.9284 3 9 -8 2 22.7544 13.9354 2 -9 -8 -2 -5.3935 11.6453 3 -2 9 8 14.0787 16.3627 1 2 -9 8 5.1975 11.1504 3 8 2 -9 8.3216 12.8384 3 8 -2 9 4.4166 12.5133 2 -9 8 2 -4.2856 14.7643 1 2 -9 8 21.9026 14.5846 2 -2 9 8 -4.1935 12.1518 2 9 8 -2 0.9687 17.0314 1 9 -8 2 8.7169 10.5436 3 2 9 -8 2.5709 15.9642 1 -2 9 -8 32.3803 14.6711 1 8 2 9 30.6574 18.1101 1 2 9 8 -13.869 15.974 1 -9 8 -2 -7.3854 14.6088 1 9 -8 -2 4.7184 11.1813 3 9 8 2 -3.2409 17.2807 1 2 9 8 3.5044 13.7516 2 8 -2 -9 10.6953 12.7598 3 -9 -8 2 0.7802 11.0252 3 -8 2 -9 26.2880 12.7202 1 -2 -9 8 8.1845 11.0254 3 2 -9 -8 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14.4053 1 9 -2 -3 19.5214 11.0902 3 3 -9 -2 54.0755 10.8680 3 2 3 9 35.5978 12.1479 2 -3 9 -2 52.0086 14.3143 1 9 2 3 56.0693 11.4137 2 -9 3 3 6.21647 8.91810 2 3 -3 9 22.7042 10.4420 2 3 9 -3 8.7835 13.3285 1 3 -3 9 6.60429 7.42006 3 -9 -3 -3 11.2460 8.0060 3 -3 3 9 6.4263 10.0845 2 -3 9 3 7.45624 8.90403 2 9 3 -3 26.8440 9.9883 3 9 -3 3 12.3124 10.9068 2 3 -9 3 4.03240 8.49178 3 -9 3 3 14.8168 9.5723 1 -3 9 3 -9.2049 11.9907 1 9 -3 3 12.7165 8.4983 3 -3 -9 -3 -6.3308 9.0571 3 3 3 -9 5.9688 10.1141 1 3 -9 3 3.5726 10.9797 2 9 3 -3 7.8507 12.8399 1 3 3 9 3.5873 13.1177 1 -3 -3 9 30.2056 11.3307 2 -3 3 -9 7.01541 9.25786 1 3 -9 -3 -5.1671 8.2314 3 -3 -9 3 3.58187 9.09037 3 3 9 3 9.76219 8.41825 2 -3 9 -3 4.9656 12.2168 1 3 9 3 -2.7618 11.8627 1 3 -3 -9 3.6010 10.2950 3 9 3 3 -4.4625 9.0321 2 9 -3 -3 3.30592 9.41594 3 -9 3 -3 10.4737 10.4478 1 9 3 3 -7.8408 12.7923 1 -3 -3 9 -2.6735 8.1583 3 -9 -3 3 8.60515 8.04323 2 3 3 9 5.2980 10.4122 2 -3 9 4 43.4082 13.7395 1 9 -4 3 9.8789 12.2221 2 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5 3 407.748 51.109 2 5 -3 9 346.234 51.517 2 9 -5 3 363.540 51.656 2 -3 -9 5 422.092 49.897 3 -5 -3 9 444.167 52.318 2 3 -9 -5 406.628 49.780 3 3 9 5 468.088 55.830 1 5 -3 -9 439.707 50.303 3 9 5 3 400.948 56.036 1 -5 3 -9 413.259 53.655 1 -9 -5 3 419.642 49.860 3 9 5 3 468.440 50.634 2 3 9 5 423.163 50.461 2 9 -5 -3 410.624 50.040 3 5 3 9 416.574 51.489 2 -9 5 -3 383.023 54.116 1 -3 9 -5 404.339 54.866 1 -9 -5 3 403.839 49.998 2 -5 -3 9 419.458 49.420 3 5 3 9 537.961 56.806 1 3 -9 6 957.683 115.296 2 6 -3 9 891.355 114.900 2 -3 9 6 968.645 121.917 1 -6 3 9 999.393 115.307 2 3 9 -6 951.267 121.451 1 3 -9 6 974.184 111.342 3 -9 6 3 913.515 121.122 1 -3 9 6 1115.20 114.97 2 -9 -6 -3 985.697 111.053 3 -9 6 3 920.588 114.602 2 9 6 -3 980.557 121.807 1 -3 -9 -6 1026.75 111.33 3 9 -6 3 950.892 115.457 2 9 -6 3 857.587 110.921 3 6 -3 -9 876.778 111.850 3 -6 -3 9 1054.92 111.32 3 -3 -9 6 1071.56 111.69 3 9 -6 -3 984.382 111.736 3 3 9 6 1040.62 122.93 1 3 -9 -6 963.961 111.524 3 9 6 3 900.837 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597.538 79.229 1 2 -4 9 689.601 72.012 3 -9 2 4 654.615 78.280 1 -2 4 9 585.981 75.742 2 9 2 -4 631.466 79.529 1 9 -2 4 663.064 75.445 2 4 9 -2 547.981 79.736 1 2 -4 9 661.287 75.465 2 -4 9 2 660.993 74.573 2 -4 -9 -2 662.507 72.889 3 -4 9 2 651.500 80.127 1 9 2 -4 563.288 72.937 3 -2 -4 -9 541.139 72.017 3 4 -9 2 585.794 75.383 2 4 -9 2 615.114 72.512 3 -9 -2 4 588.369 74.412 2 9 2 4 570.370 74.918 2 9 -2 -4 709.075 73.329 3 9 2 4 609.129 80.814 1 2 4 9 674.665 75.498 2 2 -4 -9 610.587 73.099 3 -2 -4 9 640.809 75.823 2 -2 -4 9 663.428 72.330 3 -9 2 -4 617.988 78.710 1 4 -9 -2 616.361 72.809 3 -4 -9 2 676.779 72.968 3 -2 4 -9 664.564 78.558 1 -4 9 -2 603.040 80.011 1 2 4 9 596.782 80.069 1 9 3 -4 26.2561 11.2567 3 4 -9 3 40.0051 10.3432 3 -4 9 3 48.8524 10.8262 2 3 -4 9 50.7037 9.4234 3 9 3 -4 39.1467 14.5944 1 4 9 -3 30.1017 13.7324 1 3 4 -9 40.3972 12.3491 1 9 -3 4 29.8410 9.7735 3 -4 9 3 34.7684 13.7789 1 -9 -3 -4 8.53656 8.96417 3 9 -3 4 19.8893 11.6035 2 -9 3 4 60.9941 11.5761 1 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41.5911 16.9869 1 9 4 4 76.0020 13.4328 2 4 -4 -9 54.1148 13.4305 3 4 9 4 56.7431 16.5476 1 9 -4 -4 81.4251 14.2541 3 -4 -4 9 47.8703 13.5415 2 4 4 9 53.3614 14.3128 2 -9 -4 4 73.5867 12.5775 2 9 4 4 79.9394 18.2459 1 4 -9 -4 38.0485 12.1452 3 -4 -9 4 51.5026 12.5838 3 -4 9 -4 44.8905 15.3734 1 4 9 4 75.6423 12.2639 2 -4 9 5 104.443 15.844 2 -9 -5 -4 82.1298 14.8933 3 -4 -9 -5 99.2564 15.9061 3 4 -9 5 79.5793 17.8843 2 9 -5 4 98.3200 15.1144 3 9 -5 4 62.9771 16.6042 2 4 9 -5 107.504 19.752 1 9 5 -4 162.223 20.906 1 5 -4 9 74.9935 17.0593 2 4 -9 5 94.4680 15.4463 3 -4 9 5 88.3585 19.3047 1 -9 5 4 91.5784 16.5042 2 -9 5 4 82.1542 17.5459 1 -5 4 9 103.833 17.495 2 -9 -5 4 96.7620 15.7953 2 -5 -4 9 54.0663 17.4437 2 5 4 9 75.0069 21.0296 1 -9 5 -4 51.6407 17.5566 1 5 4 9 96.0163 16.7704 2 9 5 4 88.1208 16.7636 2 -4 9 -5 87.0120 19.3602 1 -5 -4 9 129.110 16.459 3 4 9 5 111.329 16.199 2 -5 4 -9 112.918 18.544 1 -9 -5 4 82.2512 16.1749 3 9 -5 -4 108.242 16.838 3 4 9 5 72.9346 20.2253 1 -4 -9 5 63.7438 15.6229 3 5 -4 -9 115.300 17.598 3 9 5 4 61.5423 21.0104 1 4 -9 -5 86.8033 15.8885 3 -9 -6 -4 38.3574 13.3898 3 4 9 -6 55.8929 17.5818 1 9 -6 4 76.8370 12.9220 3 6 -4 9 51.9643 15.9202 2 -4 9 6 68.3149 15.1324 2 -9 6 4 39.1614 13.3200 2 9 -6 4 61.4564 16.6129 2 4 -9 6 51.9632 13.2650 3 4 -9 6 90.1687 17.2032 2 -9 6 4 61.7569 15.7949 1 9 6 -4 89.7144 19.2267 1 -6 4 9 70.2983 15.1943 2 -4 -9 -6 67.5661 13.6965 3 -4 9 6 43.9694 18.2837 1 -4 -9 6 49.5017 13.6565 3 4 9 6 59.3045 15.5811 2 -9 6 -4 61.4544 16.4063 1 9 -6 -4 41.6450 14.3783 3 -4 9 -6 59.3211 16.8709 1 9 6 4 81.5349 20.1705 1 6 4 9 68.9452 14.9005 2 -9 -6 4 60.1105 14.2693 3 -6 4 -9 84.7597 15.5749 1 -6 -4 9 64.7431 15.6604 2 6 4 9 54.6448 20.2138 1 4 9 6 45.4855 18.7936 1 -6 -4 9 46.2649 13.9051 3 6 -4 -9 66.6649 15.1296 3 9 6 4 61.9215 15.0833 2 4 -9 -6 67.7208 14.7713 3 -4 9 7 20.5419 12.7257 2 4 -9 7 10.7606 14.4560 2 4 9 -7 41.4362 16.7129 1 -9 7 4 5.0119 14.8945 1 9 -7 4 24.2418 10.7084 3 7 -4 9 19.4176 13.0331 2 4 -9 7 21.2394 11.3057 3 -9 -7 -4 16.7629 12.7621 3 -7 4 9 24.6463 12.7863 2 9 -7 4 18.4745 14.1433 2 -4 -9 -7 29.9336 12.0911 3 -9 7 4 23.6857 12.3648 2 9 7 -4 35.4998 17.7158 1 -4 9 7 5.2105 16.6068 1 4 -9 -7 15.7127 12.0510 3 -9 -7 4 8.4743 11.3599 3 7 4 9 32.4915 12.5528 2 -4 9 -7 28.6948 15.2608 1 -7 4 -9 18.2498 13.6707 1 -4 -9 7 14.9602 11.6503 3 -7 -4 9 9.8636 13.7233 2 -7 -4 9 30.4930 11.8201 3 9 7 4 2.2649 17.0823 1 7 4 9 1.0723 18.0327 1 -9 7 -4 27.0067 14.4176 1 4 9 7 8.8302 17.8920 1 7 -4 -9 35.3952 13.9805 3 4 9 7 -0.3816 14.1987 2 9 -7 -4 41.5395 13.7918 3 4 9 -8 133.638 23.621 1 9 -8 4 65.3941 21.0660 2 -4 9 8 90.5360 23.5624 1 -8 4 9 156.451 21.357 2 9 8 -4 90.9889 23.9191 1 9 -8 4 131.288 18.129 3 -9 8 4 61.5376 21.9701 1 4 -9 8 101.631 20.848 2 -4 9 8 101.220 19.693 2 8 -4 9 94.8581 21.1696 2 4 -9 8 102.172 18.126 3 -9 8 4 115.525 19.263 2 8 -4 -9 87.2535 20.0583 3 4 9 8 112.377 24.883 1 -8 4 -9 128.135 21.262 1 -8 -4 9 82.5132 20.3482 2 4 -9 -8 89.0452 19.8237 3 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5 9 17.2727 14.6657 2 -8 -5 9 20.4545 13.6083 3 -5 9 -8 11.2920 15.8135 1 5 9 8 50.4377 16.5059 2 5 9 8 22.1623 20.5910 1 9 -8 -5 14.6104 13.9108 3 8 5 9 35.5882 20.4894 1 -5 -9 8 10.4661 12.4613 3 -8 -5 9 16.3227 16.5747 2 -9 -8 5 11.8170 12.8466 3 8 -5 -9 4.5680 15.2263 3 5 -9 -8 8.7791 14.0414 3 -8 5 -9 -4.5708 14.6010 1 9 8 5 15.0305 18.6417 1 -9 8 -5 20.3883 16.5952 1 8 5 9 15.6611 14.5540 2 -6 -9 0 72.8727 13.0979 3 6 -9 0 55.9247 12.5188 3 0 -6 9 78.1441 14.2761 2 9 0 -6 68.6913 14.0127 3 6 9 0 67.0614 17.8339 1 0 6 -9 53.6600 14.6525 1 0 -6 -9 71.2785 13.7337 3 9 0 6 44.4493 13.8957 2 0 -6 9 50.7120 11.8832 3 9 0 6 46.5377 17.5199 1 6 -9 0 47.2672 13.8515 2 0 6 9 37.7855 17.0444 1 -9 0 6 42.3663 12.7325 2 -6 9 0 54.1584 16.6011 1 0 6 9 53.0743 14.8045 2 6 -9 1 65.0434 12.2118 3 -1 6 9 7.6800 14.8562 1 6 9 -1 22.6582 14.3191 1 9 -1 6 3.3968 14.3401 1 -1 -6 -9 17.8317 10.9298 3 -6 9 1 43.3383 14.8911 1 9 1 -6 21.9231 11.5397 3 1 6 -9 42.9290 13.5840 1 -1 6 9 41.0378 12.5334 2 9 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173.684 21.985 3 -9 -2 6 147.614 22.184 2 6 -9 -2 148.409 21.276 3 9 -2 -6 141.148 22.507 3 -2 -6 9 144.903 20.844 3 6 9 2 175.984 26.525 1 2 6 9 146.095 26.468 1 2 6 9 145.357 23.030 2 -2 -6 9 2.7213 20.6997 2 -9 2 -6 146.182 23.235 1 9 2 6 152.804 27.081 1 -6 9 3 993.312 117.531 2 3 6 -9 1008.71 123.70 1 -3 6 9 1043.58 124.77 1 6 -9 3 1037.51 118.32 2 -6 9 3 1103.08 125.09 1 3 -6 9 1061.92 118.11 2 9 3 -6 979.679 114.488 3 6 -9 3 1086.56 113.99 3 9 -3 6 882.265 117.958 2 6 9 -3 1080.90 124.55 1 -9 3 6 990.006 117.601 2 -6 -9 -3 919.813 114.131 3 -3 6 9 975.241 117.838 2 3 -6 9 1024.12 113.51 3 -3 -6 9 988.939 113.853 3 9 3 6 819.827 125.172 1 9 -3 -6 999.930 114.668 3 -6 -9 3 978.576 114.219 3 3 6 9 1000.22 117.91 2 -6 9 -3 1005.88 124.81 1 9 3 6 869.329 117.495 2 6 -9 -3 1091.65 114.34 3 -3 6 -9 1087.70 124.10 1 3 6 9 987.512 125.633 1 -3 -6 9 967.398 117.663 2 -9 -3 6 1016.57 117.46 2 -9 3 -6 961.306 124.141 1 6 9 3 898.197 124.988 1 3 -6 -9 1035.80 114.57 3 -4 6 9 94.2260 16.3947 2 -9 4 6 38.4577 14.3617 2 4 6 -9 69.3801 17.2901 1 6 -9 4 53.3493 12.6288 3 -6 -9 -4 79.4327 14.9693 3 -6 9 4 82.8651 18.7082 1 -6 9 4 67.4990 15.0536 2 4 -6 9 71.7542 14.0610 3 6 -9 4 71.1785 17.5339 2 4 -6 9 72.3603 16.5286 2 6 9 -4 107.167 17.869 1 9 -4 6 91.2488 16.8175 2 9 -4 6 92.7423 13.6772 3 -9 -4 6 58.2009 14.9515 2 -6 9 -4 59.2606 17.2392 1 4 6 9 70.4417 15.2725 2 9 -4 -6 68.5268 15.5791 3 -4 -6 9 64.2293 15.7638 2 9 4 6 57.3973 15.2575 2 -4 6 -9 63.0779 16.5478 1 -9 -4 6 73.4621 14.2735 3 9 4 6 51.3178 19.4031 1 4 -6 -9 56.5932 15.5452 3 -4 -6 9 63.6378 14.2812 3 -9 4 -6 43.3591 15.6277 1 -6 -9 4 69.3482 14.6612 3 6 9 4 33.7395 18.8047 1 6 -9 -4 55.7663 14.6214 3 4 6 9 90.9822 21.5036 1 6 -9 5 45.1073 16.0810 2 -6 9 5 74.1599 15.2572 2 9 -5 6 73.2617 16.7445 2 -6 9 5 46.3036 18.6685 1 -9 5 6 49.8597 14.8902 2 9 -5 6 63.9328 13.8789 3 5 -6 9 78.2443 16.6839 2 6 -9 5 82.7605 13.9615 3 5 -6 9 72.8049 13.9745 3 6 9 -5 100.253 18.389 1 -6 -9 -5 106.681 15.678 3 -5 6 9 39.7247 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38.367 1 2 -10 3 252.442 35.722 3 -2 -10 -3 297.523 35.921 3 2 10 -3 254.449 39.904 1 -10 -3 -2 284.302 35.248 3 -3 -2 10 281.155 35.140 3 3 2 10 276.017 40.887 1 2 10 3 338.869 41.433 1 -3 -2 10 228.239 37.663 2 -2 10 -3 247.149 40.379 1 2 10 3 278.016 35.574 2 -2 -10 3 285.776 36.081 3 2 -10 -3 319.174 36.409 3 -10 3 -2 293.552 39.459 1 -10 -3 2 271.864 36.262 2 3 2 10 306.795 38.143 2 3 -2 -10 301.797 36.365 3 10 3 2 272.343 40.718 1 -3 2 -10 276.180 38.427 1 10 -3 -2 329.844 37.851 2 10 -3 -2 322.193 36.691 3 10 3 2 249.409 36.449 2 -10 4 2 117.632 17.691 1 10 4 -2 74.7580 19.4590 1 2 -10 4 95.4015 15.8393 3 -2 10 4 60.8331 19.0513 1 2 -10 4 69.1132 16.4010 2 -2 10 4 102.595 15.987 2 -10 -4 -2 94.7813 15.1708 3 2 10 -4 126.730 19.991 1 4 -2 10 81.9352 16.2627 2 -2 -10 -4 84.5717 15.9672 3 10 -4 2 81.3772 17.5826 2 10 -4 2 65.7690 14.5584 3 -4 2 10 98.8519 18.0119 2 -10 -4 2 64.4055 14.8285 3 2 -10 -4 123.978 16.803 3 10 -4 -2 71.6026 15.5231 3 -4 -2 10 98.5350 18.1528 2 -10 4 -2 89.1072 18.4494 1 2 10 4 88.8988 15.7719 2 -2 10 -4 106.085 19.714 1 2 10 4 124.928 20.285 1 4 2 10 68.7089 20.0363 1 4 -2 -10 48.2484 15.7890 3 -4 2 -10 98.6056 16.7029 1 -2 -10 4 88.7305 16.0024 3 -10 -4 2 123.776 15.589 2 10 -4 -2 75.2140 16.8195 2 -4 -2 10 99.6347 14.7844 3 10 4 2 88.3135 16.3006 2 10 4 2 86.6998 20.5915 1 4 2 10 146.293 18.508 2 5 -2 10 81.7329 19.7549 2 -2 10 5 124.293 23.267 1 2 -10 5 87.8288 19.5289 2 -5 2 10 97.7607 20.0442 2 -2 -10 -5 113.826 18.219 3 10 -5 2 148.845 21.545 2 -2 10 5 120.916 18.353 2 -10 -5 -2 139.051 18.255 3 2 10 -5 103.815 21.760 1 2 -10 5 131.007 19.043 3 -10 5 2 159.662 20.874 1 10 5 -2 120.996 22.598 1 10 -5 2 128.347 18.024 3 2 -10 -5 106.156 18.707 3 -10 5 -2 51.2575 20.4156 1 -10 -5 2 12.9680 16.9012 3 -2 10 -5 101.750 22.194 1 10 5 2 176.618 24.739 1 2 10 5 102.678 19.088 2 10 5 2 143.572 19.257 2 5 2 10 165.011 20.886 2 5 2 10 174.234 25.541 1 -2 -10 5 121.596 18.642 3 2 10 5 141.811 22.887 1 -5 2 -10 129.650 20.181 1 5 -2 -10 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10 4 -3 228.283 34.080 1 -4 3 10 251.213 32.526 2 3 -10 4 163.069 31.058 2 -3 10 4 260.067 30.540 2 10 -4 3 251.104 29.585 3 10 -4 3 184.505 31.996 2 4 -3 10 201.452 31.679 2 -3 -10 -4 221.378 29.798 3 3 -10 4 218.013 29.681 3 -10 -4 -3 251.020 29.294 3 -10 4 3 218.576 30.810 2 -10 4 3 239.258 32.278 1 -3 10 4 243.908 34.665 1 3 10 -4 221.886 33.650 1 -4 3 -10 270.195 32.662 1 4 3 10 248.786 32.304 2 10 -4 -3 232.429 30.631 3 -3 -10 4 254.312 30.585 3 -10 -4 3 236.497 30.297 3 -4 -3 10 280.632 33.315 2 -10 -4 3 240.882 30.051 2 -3 10 -4 250.135 34.848 1 4 3 10 213.692 35.194 1 -4 -3 10 223.498 29.302 3 3 -10 -4 229.266 30.245 3 4 -3 -10 232.594 30.525 3 10 4 3 200.867 30.719 2 10 4 3 219.472 35.335 1 3 10 4 207.132 34.180 1 -10 4 -3 222.275 33.374 1 -3 10 5 289.392 41.954 1 -10 5 3 291.193 40.179 1 -3 10 5 364.008 38.218 2 3 -10 5 303.190 36.897 3 10 -5 3 287.917 36.256 3 10 -5 3 259.205 38.591 2 -10 -5 -3 329.343 36.440 3 -10 5 3 245.236 37.672 2 5 -3 10 312.476 39.070 2 -5 3 10 311.938 39.144 2 10 5 -3 294.254 41.264 1 -3 -10 -5 340.100 37.362 3 3 -10 5 263.915 38.189 2 3 10 -5 289.648 41.212 1 3 -10 -5 279.861 36.981 3 5 3 10 304.281 38.920 2 -5 -3 10 300.715 39.677 2 5 3 10 330.930 43.586 1 10 -5 -3 297.749 37.418 3 -10 5 -3 307.984 40.972 1 10 5 3 280.683 37.801 2 10 5 3 294.205 42.702 1 5 -3 -10 279.551 37.514 3 -3 -10 5 303.149 37.253 3 -10 -5 3 236.267 36.777 3 -5 -3 10 291.739 36.508 3 -3 10 -5 301.780 41.612 1 3 10 5 279.964 42.373 1 -5 3 -10 257.953 39.534 1 10 6 -3 117.020 21.312 1 3 -10 6 12.4048 16.8965 2 -3 -10 -6 88.1287 15.9947 3 3 10 -6 107.947 20.700 1 3 -10 6 82.4689 16.0119 3 10 -6 3 57.4983 17.0695 2 -10 -6 -3 92.2543 15.8391 3 6 -3 10 70.7784 17.6547 2 -10 6 3 73.5044 18.0586 1 -10 6 3 37.3111 15.2373 2 10 -6 3 97.9415 15.4833 3 -3 10 6 95.7018 16.9533 2 -6 3 10 128.474 18.984 2 -3 10 6 144.288 22.468 1 -6 -3 10 110.923 19.980 2 -10 6 -3 101.246 19.509 1 -6 3 -10 106.579 18.904 1 -3 -10 6 29.0981 15.0066 3 10 6 3 107.275 22.044 1 6 3 10 85.5978 17.3035 2 3 10 6 35.5460 20.8274 1 -10 -6 3 106.797 16.767 3 3 -10 -6 68.9624 15.8855 3 6 -3 -10 92.8055 17.5673 3 -6 -3 10 125.245 16.191 3 3 10 6 70.9802 17.0611 2 -3 10 -6 96.4835 20.8514 1 10 -6 -3 74.0677 16.5147 3 6 3 10 95.0064 22.2008 1 10 7 -3 50.3981 20.5645 1 10 -7 3 52.8117 13.0031 3 -3 -10 -7 32.2946 13.7984 3 -10 -7 -3 57.1498 14.0479 3 3 -10 7 19.4175 15.9538 2 -7 3 10 67.0510 16.2554 2 3 -10 7 45.6638 13.2277 3 -10 7 3 45.1978 16.5082 1 10 -7 3 27.0371 16.1273 2 -10 7 3 72.4738 14.7947 2 -3 10 7 45.3170 14.0688 2 7 -3 10 65.7364 15.9590 2 3 10 -7 25.3452 18.4831 1 -3 10 7 24.4663 19.2964 1 -10 -7 3 68.5185 14.3904 3 3 10 7 42.0656 15.8632 2 10 7 3 43.5340 19.9622 1 7 3 10 21.7489 19.8154 1 3 10 7 54.1324 18.8783 1 -3 -10 7 32.3159 13.5502 3 3 -10 -7 28.0950 13.7840 3 -7 3 -10 46.6249 15.8190 1 -3 10 -7 36.1071 17.5110 1 10 -7 -3 45.1682 14.2214 3 -7 -3 10 44.3665 12.4956 3 -10 7 -3 46.9171 16.7180 1 -7 -3 10 7.6166 15.4520 2 7 -3 -10 20.3034 15.0489 3 7 3 10 35.9567 14.4985 2 10 8 -3 231.279 35.586 1 8 -3 10 195.756 31.242 2 -8 3 10 241.063 32.038 2 -3 10 8 225.907 34.367 1 -3 10 8 227.438 31.401 2 3 -10 8 243.683 29.377 3 3 -10 8 227.220 32.028 2 10 -8 3 192.321 31.952 2 -10 8 3 226.457 33.150 1 -3 -10 -8 204.441 29.639 3 -10 -8 -3 216.167 29.329 3 10 -8 3 240.030 29.134 3 3 10 -8 213.157 34.590 1 -10 8 3 167.294 29.532 2 8 3 10 169.266 30.563 2 -8 -3 10 186.350 28.459 3 8 -3 -10 198.135 30.329 3 -3 10 -8 212.483 33.534 1 -10 -8 3 174.444 28.865 3 -8 -3 10 203.378 31.879 2 -10 8 -3 227.954 33.976 1 10 -8 -3 212.570 29.703 3 3 -10 -8 241.738 30.495 3 10 8 3 256.425 35.783 1 -8 3 -10 197.292 32.528 1 3 10 8 189.030 30.995 2 3 10 8 234.419 35.943 1 -3 -10 8 259.886 29.875 3 8 3 10 152.653 35.165 1 10 9 -3 301.501 41.813 1 3 10 -9 313.251 40.692 1 -10 9 3 256.580 35.071 2 10 -9 3 215.845 33.384 3 9 -3 10 285.409 37.265 2 3 -10 9 183.188 36.458 2 -10 -9 -3 248.791 34.838 3 3 -10 9 277.999 34.457 3 -9 3 10 181.494 35.922 2 10 -9 3 305.533 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2 -5 10 111.998 20.924 2 5 10 2 97.7241 22.7978 1 -2 5 -10 124.397 20.480 1 -10 2 -5 153.823 21.268 1 -2 -5 10 111.714 20.742 2 2 5 10 151.679 21.578 2 2 -5 -10 101.986 19.366 3 -5 10 -2 86.7092 22.6468 1 10 2 5 152.999 25.182 1 -2 -5 10 130.405 18.558 3 5 -10 -2 112.771 18.995 3 -10 -2 5 120.674 19.095 2 10 2 5 82.5517 19.2921 2 10 -2 -5 106.108 19.572 3 2 5 10 104.035 23.349 1 -5 -10 2 130.270 19.676 3 5 10 -3 286.768 42.308 1 5 -10 3 303.686 39.648 2 -3 5 10 340.629 40.393 2 10 3 -5 319.827 38.151 3 -5 -10 -3 375.360 38.610 3 5 -10 3 336.620 38.081 3 3 -5 10 337.988 36.867 3 3 -5 10 267.528 39.334 2 -10 3 5 286.440 38.953 2 10 -3 5 185.609 38.354 2 -5 10 3 327.390 38.739 2 10 3 -5 470.475 43.626 1 -5 10 3 283.840 42.825 1 10 -3 5 356.559 37.342 3 -3 -5 10 233.627 36.748 3 10 3 5 291.464 38.720 2 3 5 10 262.227 42.316 1 -3 -5 10 301.285 39.930 2 5 10 3 228.686 42.127 1 -10 3 -5 304.112 41.115 1 -10 -3 5 314.014 38.441 2 -3 5 -10 266.689 40.150 1 3 5 10 346.263 40.112 2 3 -5 -10 294.289 38.339 3 -5 10 -3 309.486 42.053 1 -5 -10 3 307.395 37.817 3 10 3 5 224.834 42.544 1 5 -10 -3 280.706 37.535 3 10 -3 -5 303.974 38.421 3 4 -5 10 50.3183 15.7341 2 10 -4 5 74.2012 13.8885 3 5 -10 4 47.1347 16.2498 2 -4 5 10 36.2211 14.9047 2 -5 10 4 87.3045 14.8936 2 -5 -10 -4 59.9499 14.4796 3 10 -4 5 50.4215 16.1760 2 5 -10 4 42.1826 13.1400 3 -5 10 4 31.0900 17.9932 1 -10 4 5 83.7652 14.6338 2 10 4 -5 65.2530 19.4359 1 5 10 -4 46.5375 17.1853 1 4 -5 -10 68.9705 16.4446 3 -4 5 -10 45.8458 15.4960 1 5 -10 -4 24.0436 12.9292 3 10 -4 -5 40.5547 14.9097 3 4 5 10 55.8504 19.2666 1 -10 -4 5 73.4332 14.2859 3 -4 -5 10 72.8869 13.6791 3 4 5 10 28.3854 14.9400 2 -5 -10 4 59.2400 14.0967 3 -4 -5 10 59.9672 16.7308 2 -10 -4 5 79.5404 15.0525 2 10 4 5 82.5696 20.7052 1 10 4 5 37.4747 14.8219 2 -5 10 -4 33.6300 16.7542 1 5 10 4 25.6573 17.8676 1 -10 4 -5 46.2536 15.6719 1 -5 -10 -5 26.2058 13.2344 3 5 -10 5 30.8661 11.5572 3 5 -10 5 24.6987 14.0956 2 -5 5 10 10.4612 12.9765 2 -10 5 5 36.1602 12.6237 2 10 -5 5 12.4523 13.5163 2 10 5 -5 23.4697 19.1260 1 5 10 -5 -5.1561 15.6118 1 10 -5 5 23.7121 12.4643 3 -5 10 5 24.0728 17.9995 1 -5 10 5 27.2621 12.1907 2 5 -5 10 13.9058 14.1679 2 -5 -5 10 39.2316 15.2668 2 -5 -5 10 18.6076 11.4114 3 -10 5 -5 1.3367 14.5697 1 10 -5 -5 24.0025 13.6105 3 5 5 10 25.2072 18.3721 1 5 5 10 21.5776 13.3886 2 -5 10 -5 2.2082 15.6098 1 5 10 5 61.1700 18.0117 1 10 5 5 42.1370 14.1117 2 10 5 5 31.1974 18.6042 1 5 -5 -10 11.2608 13.6641 3 -5 -10 5 39.8002 13.3364 3 -10 -5 5 -1.9850 12.5851 3 5 -10 -5 15.4019 12.1590 3 -5 5 -10 -5.2163 13.6458 1 10 -6 5 11.7797 11.9912 3 -5 10 6 23.0705 12.8756 2 -10 6 5 12.2346 12.5050 2 5 10 -6 14.4146 17.9864 1 10 -6 5 6.1969 14.1819 2 -5 10 6 38.2761 18.4834 1 5 -10 6 7.8115 11.9018 3 -5 -10 -6 24.5866 13.4201 3 6 -5 10 35.4863 15.2298 2 -6 5 10 3.9972 13.7680 2 10 6 -5 34.7599 19.7249 1 5 -10 6 17.7775 14.8039 2 6 -5 -10 25.3346 14.8005 3 10 -6 -5 18.1239 13.9082 3 10 6 5 8.0388 18.7544 1 -6 -5 10 5.9757 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